Structural Attributes in Cold Recycled Asphalt Mixes: Microstructure Insights

Document Type : Original Article

Authors
1 Department of Civil Engineering, Iran University of Science and Technology (IUST), Tehran, Iran.
2 M.Sc., Student, Department of Civil Engineering, Iran University of Science and Technology (IUST), Tehran, Iran.
3 Ph.D., Student, Department of Civil Engineering, Iran University of Science and Technology (IUST), Tehran, Iran.
Abstract
This study provides a comprehensive exploration of the microstructure characteristics of cold recycled asphalt mixes, with a primary focus on their environmental benefits. Utilizing a suite of analytical techniques including Optical Microscopy, Scanning Electron Microscopy, Transmission Electron Microscopy, X-ray diffraction, and Scanning Force Microscopy, the study delves into four pivotal microstructure facets: air voids and coarse aggregates, uniformity index, the impact of diverse additives, and the process of augmenting initial strength. The findings reveal that several factors, notably aggregate grading and compaction methodology, exert a notable influence on the microstructure of cold recycled mixes. Specifically, transitioning from fine to coarse grading amplifies void space within the cold asphalt mix. Moreover, both compaction methods and aggregate grading significantly alter the size and distribution of air voids. The study establishes that as grading shifts from fine to coarse, the uniformity of cold recycled asphalt mixes experiences a gradual decline. Additionally, the Superpave Gyratory compaction method emerges as the most effective among the three compaction methods considered. Furthermore, the investigation assesses the impact of diverse additives on microstructure and overall performance. Notably, optimal cement content for cold recycled asphalt, when using bitumen emulsion, is found to be in the range of 1-2%, ensuring resistance against cracking at low temperatures. In general, this research indicates the importance of considering the microstructure in the design and evaluation of cold recycled asphalt mixtures, which can help to develop sustainable asphalt mixtures
Keywords

-Abbasnejad, S. Y., & Modarres, A., (2020). Effect of setting accelerator additive on short-and long-term properties of cold recycled mixture containing bitumen emulsion–cement composites. Road Materials and Pavement Design, 21(7), 1932-1954.
-B.D. Cullity, S. R. S. (2014). Elements of X-Ray Diffraction (Third ed.). Pearson Education Limited. http://gen.lib.rus.ec/book/index.php?md5=a334b668e19ba9a86c96937522a7dabf
-Bharat Bhushan (auth.), P. B. B. e., (2010). Springer Handbook of Nanotechnology (3 ed.). Springer-Verlag Berlin Heidelberg. http://gen.lib.rus.ec/book/index.php?md5=d2a40c862f84d366ec521203953980a3
-BuczyƄski, P., Šrámek, J., & Mazurek, G., (2023). The Influence of Recycled Materials on Cold Mix with Foamed Bitumen Properties. Materials, 16(3), 1208.
-Chen, T., Ma, T., Huang, X., Ma, S., Tang, F., & Wu, S., (2020). Microstructure of synthetic composite interfaces and verification of mixing order in cold-recycled asphalt emulsion mixture. Journal of Cleaner Production, 263, 121467.
-David B. Williams, C. B. C., (2009). Transmission electron microscopy: a textbook for materials science (2nd ed ed.). Springer.
-David Brandon, W. D. K., (2008). Microstructural Characterization of Materials. Wiley.
-Di Gianfrancesco, A., (2017). 8 - Technologies for chemical analyses, microstructural and inspection investigations. In A. Di Gianfrancesco (Ed.), Materials for Ultra-Supercritical and Advanced Ultra-Supercritical Power Plants.  197-245.
 Woodhead Publishing.
-Farooq, M. A., & Mir, M. S., (2017). Use of reclaimed asphalt pavement (RAP) in warm mix asphalt (WMA) pavements: a review. Innovative Infrastructure Solutions, 2(1), 10.     doi.org/10.1007/s41062-017-0058-7
-Gao, L., Ni, F., Luo, H., & Charmot, S., (2015). Characterization of air voids in cold in-place recycling mixtures using X-ray computed tomography. Construction and Building Materials, 84, 429-436.
-Gu, F., Ma, W., West, R. C., Taylor, A. J., & Zhang, Y., (2019). Structural performance and sustainability assessment of cold central-plant and in-place recycled asphalt pavements: A case study. Journal of Cleaner Production, 208, 1513-1523.
-Hoy, M., Horpibulsuk, S., & Arulrajah, A., (2016). Strength development of recycled asphalt pavement–fly ash geopolymer as a road construction material. Construction and Building Materials, 117, 209-219.
-Hull D., B. D. J., (2011). Introduction to Dislocations (5ed. ed.).
-Jin, D., Ge, D., Chen, S., Che, T., Liu, H., Malburg, L., & You, Z., (2021). Cold in-place recycling asphalt mixtures: Laboratory performance and preliminary ME design analysis. Materials, 14(8), 2036.
-Joseph Goldstein, D. E. N., David C. Joy, Charles E. Lyman, Patrick Echlin, Eric Lifshin, Linda Sawyer, J.R. Michael. (2003). Scanning Electron Microscopy and X-ray Microanalysis (3rd ed.). Springer. http://gen.lib.rus.ec/book/index.php?md5=2b40548ad6465ef47b9d601aaeb80900
-Kong, L., Lu, Z., He, Z., Shen, Z., Xu, H., Yang, K., & Yu, L., (2022). Characterization of crack resistance mechanism of fiber modified emulsified asphalt cold recycling mixture based on acoustic emission parameters. Construction and Building Materials, 327, 126939.
-Leng, Y., (2013). Materials Characterization: Introduction to Microscopic and Spectroscopic Methods (2nd edition ed.). Wiley-VCH.
-Li, Q., Zhu, C., Zhang, H., & Zhang, S., (2022). Evaluation on long-term performance of emulsified asphalt cold recycled mixture incorporating fly ash by mechanistic and microscopic characterization. Construction and Building Materials, 319, 126120.
-Li, X., Wen, H., Edil, T. B., Sun, R., & VanReken, T. M., (2013). Cost, energy, and greenhouse gas analysis of fly ash stabilised cold in-place recycled asphalt pavement. Road Materials and Pavement Design, 14(3), 537-550.
-Li, Y., Lyv, Y., Fan, L., & Zhang, Y., (2019). Effects of cement and emulsified asphalt on properties of mastics and 100% cold recycled asphalt mixtures. Materials, 12(5), 754.
-Li, Z., Hao, P., Liu, H., & Xu, J., (2019). Effect of cement on the strength and microcosmic characteristics of cold recycled mixtures using foamed asphalt. Journal of Cleaner Production, 230, 956-965.
-Lin, J., Hong, J., & Xiao, Y., (2017). Dynamic characteristics of 100% cold recycled asphalt mixture using asphalt emulsion and cement. Journal of Cleaner Production, 156, 337-344.
-Lin, J., Huo, L., Xiao, Y., Xu, F., & Pan, P., (2020). Long-term performance characteristics and interface microstructure of field cold recycled asphalt mixtures. Construction and Building Materials, 259, 120406.
-Lin, J., Huo, L., Xu, F., Xiao, Y., & Hong, J., (2018). Development of microstructure and early-stage strength for 100% cold recycled asphalt mixture treated with emulsion and cement. Construction and Building Materials, 189, 924-933.
-Lin, J., Wei, T., Hong, J., Zhao, Y., & Liu, J., (2015). Research on development mechanism of early-stage strength for cold recycled asphalt mixture using emulsion asphalt. Construction and Building Materials, 99, 137-142.
-Lin, J., Xia, Y., Huo, L., Hong, J., Zhu, X., & Wu, S., (2022). Fatigue crack evolution and characteristic of cold recycled asphalt mixture in different dimensions. Construction and Building Materials, 325, 126818.
-Lin, J., Zhong, C., Hong, J., Zhu, X., & Xiao, Y., Investigation on Performance and Microscopic Mechanism of Cold Recycled Mixture with Geopolymer and Asphalt Emulsion. Available at SSRN 4549305.
-Liu, Z., Sun, L., Zhai, J., & Huang, W., (2022). A review of design methods for cold in-place recycling asphalt mixtures: Design processes, key parameters, and evaluation. Journal of Cleaner Production, 133530.
-Lu, K., (2014). Nanomaterials. Making strong nanomaterials ductile with gradients. Science, 345(6203), 1455-1456.
-Lyu, Z., Shen, A., Qin, X., Yang, X., & Li, Y., (2019). Grey target optimization and the mechanism of cold recycled asphalt mixture with comprehensive performance. Construction and Building Materials, 198, 269-277.
-Ma, T., Wang, H., Zhao, Y., Huang, X., & Pi, Y., (2015). Strength mechanism and influence factors for cold recycled asphalt mixture. Advances in Materials Science and Engineering, 2015.
-Ma, Y., Polaczyk, P., Hu, W., Zhang, M., & Huang, B. (2021). Quantifying the effective mobilized RAP content during hot in-place recycling techniques. Journal of Cleaner Production, 314, 127953.
doi.org/https://doi.org/10.1016/j.jclepro.2021.127953
-Ma, Y., Polaczyk, P., Xiao, R., Jiang, X., Zhang, M., Liu, Y., & Huang, B. (2022). Influence of mobilized RAP content on the effective binder quality and performance of 100% hot in-place recycled asphalt mixtures. Construction and Building Materials, 342, 127941. doi.org/https://doi.org/10.1016/j.conbuildmat.2022.127941
-Ma, Y., Wang, S., Zhou, H., Hu, W., Polaczyk, P., & Huang, B. (2022). Recycled polyethylene and crumb rubber composites modified asphalt with improved aging resistance and thermal stability. Journal of Cleaner Production, 334, 130102. doi.org/https://doi.org/10.1016/j.jclepro.2021.130102
-Meyers, M. A., Mishra, A., & Benson, D. J. (2006). Mechanical properties of nanocrystalline materials. Progress in materials science, 51(4), 427-556.
-Mokobi, F. (2022). Atomic Force Microscope (AFM)- Definition, Principle, Parts, Uses. https://microbenotes.com/atomic-force-microscope-afm/
-Pantini, S., Borghi, G., & Rigamonti, L., (2018). Towards resource-efficient management of asphalt waste in Lombardy region (Italy): Identification of effective strategies based on the LCA methodology. Waste Management, 80, 423-434. doi.org/10.1016/j.wasman.2018.09.035
-Peter Eaton, P. W., (2010). Atomic Force Microscopy. Oxford University Press, USA. http://gen.lib.rus.ec/book/index.php?md5=22d557229da2b0792a000372220c2b7a
-Pi, Y., Huang, Z., Pi, Y., Li, G., & Li, Y., (2019). Composition design and performance evaluation of emulsified asphalt cold recycled mixtures. Materials, 12(17), 2682.
-Pi, Y., Li, Y., Pi, Y., Huang, Z., & Li, Z., (2019). Strength and micro-mechanism analysis of cement-emulsified asphalt cold recycled mixture. Materials, 13(1), 128.
-Santos, J., Flintsch, G., & Ferreira, A., (2017). Environmental and economic assessment of pavement construction and management practices for enhancing pavement sustainability. Resources, Conservation and Recycling, 116, 15-31. doi.org/10.1016/j.resconrec.2016.08.025
-Taheri-Shakib, J., & Al-Mayah, A. (2023). A review of microstructure characterization of asphalt mixtures using computed tomography imaging: Prospects for properties and phase determination. Construction and Building Materials, 385, 131419.
-Taherkhani, H., & Noorian, F. (2020). Comparing the effects of waste engine and cooking oil on the properties of asphalt concrete containing reclaimed asphalt pavement (RAP). Road Materials and Pavement Design, 21(5), 1238-1257. doi.org/10.1080/14680629.2018.1546220
-Wang, D., Guo, T., Chang, H., Yao, X., Chen, Y., & Wang, T., (2021). Research on the performance of regenerant modified cold recycled mixture with asphalt emulsions. Sustainability, 13(13), 7284.
-Wang, J., Qin, Y., Xu, J., Chang, R., & Liu, L., (2022). Microscale Property Evaluation of the Interface between Cement Emulsified Asphalt and Aged Asphalt in Emulsified Asphalt Cold Recycled Mixture. Journal of Materials in Civil Engineering, 34(6), 04022086.
-Wang, M., Huo, T., Xing, C., & Wang, Y., (2023). Influence of Fiber Mixing Process on the Cracking Resistance of Cold Recycled Asphalt Mixture. Applied Sciences, 13(2), 999.
-Wang, Z., Dai, N., Wang, X., Li, G., & Guo, H., (2020). Early-stage road property improvements of cold recycled asphalt emulsion mixture with microwave technology. Journal of Cleaner Production, 263, 121451.
-Xiao, F., Yao, S., Wang, J., Li, X., & Amirkhanian, S., (2018). A literature review on cold recycling technology of asphalt pavement. Construction and Building Materials, 180, 579-604.
-Yang, Y., Yang, Y., & Qian, B., (2019). Performance and microstructure of cold recycled mixes using asphalt emulsion with different contents of cement. Materials, 12(16), 2548.
-Yao, X., Tan, L., & Xu, T., (2022). Preparation, properties and compound modification mechanism of waterborne epoxy resin/styrene butadiene rubber latex modified emulsified asphalt. Construction and Building Materials, 318, 126178.
-Yao, X., Xu, H., & Xu, T., (2022). Syncretization mechanism between emulsified asphalt and aged asphalt in cold recycled asphalt mixture using developed demulsification-dehydration method. Construction and Building Materials, 326, 126860.
-Yu, B., Gu, X., Ni, F., & Gao, L., (2018). Microstructure characterization of cold in-place recycled asphalt mixtures by X-ray computed tomography. Construction and Building Materials, 171, 969-976.